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Data supporting a provisional American Society for Testing and Materials (ASTM) method for metalworking fluids, part I: a solvent blend with wide-ranging ability to dissolve metalworking fluids.
Glaser RA; Shulman S; Klinger P
J Test Eval 1999 Mar; 27(2):171-174
Data are presented to support modification to a provisional American Society for Testing and Materials (ASTM) sampling and analytical technique for metalworking fluids (ASTM P-42-97). The method, tentatively recommended by ASTM Subcommittee D-22.04, involves collection of the aerosolized fluid on a filter and separation of the fluid from co-sampled particulate matter via solvent extraction of that fluid from the filter. The solubilities of nine metalworking fluids were tested in seven solvents: acetone, dichloromethane, ethyl acetate, isopropanol, methanol, toluene, water, and three solvent blends: dichloromethane: methanol, dichloromethane:methanol:toluene, and dichloro-methane:methanol:hexane. A ternary blend of dichloromethane: methanol:toluene (1:1:1) was found to dissolve samples of the four classes of metalworking fluids within about 1 min.
Analytical-chemistry; Analytical-methods; Analytical-processes; Solvents; Metalworking; Metalworking-fluids; Metalworking-industry; Synthetic-materials; Metalworking-fluids; Quality-control; Exposure-levels; Particulate-dust; Particulate-sampling-methods; Particulates; Milling-industry; Author Keywords: metalworking fluids; ASTM analytical method; ternary solvent; solubility studies
Issue of Publication
Journal of Testing and Evaluation
Page last reviewed: September 2, 2020
Content source: National Institute for Occupational Safety and Health Education and Information Division