NIOSH Backup Data Report Nitroethane S219 (Set 4).
NIOSH 1978 Jan:21 pages
A protocol for validation of a method for collection analysis of nitroethane (79243) was tested and described. For validation, the absolute total air-monitoring error should be less than 25 percent in at least 95 percent of the samples analyzed at the level of the OSHA standard. The validation consisted of determining the breakthrough capacity of XAD-2 resin at high relative humidity; analyzing 18 samples spiked with nitroethane to represent a sample volume equal to 3 liters; analyzing 18 samples collected from dynamically generated test atmospheres; testing of the storage stability of collected samples; and assessing the precision and accuracy of the method. The method passed all the program requirements.
NIOSH-Author; NIOSH-Analytical-Method; Analytical-Method; Standards-Completion-Program; SCP; Standards; Sampling; Set-4; Nitro-compounds; Air-contaminants; Instrumentation; Backup-data;
Division of Physical Sciences and Engineering, NIOSH, Cincinnati, Ohio, 21 pages, 3 references