NIOSH Analytical Method, Stibine, Backup Data Report, S243 (Set 2).
NIOSH 1977 Jul:27 pages
The backup data report is given for validating the method for determining stibine (7803523) in the air. Samples were analyzed regarding evaluation of the Rhodamine-B method of analysis for antimony (7440360), development of a method for independent verification of the stibine concentration, collection by mercuric- chloride coated silica gel, collection efficiency, storage stability, and precision and accuracy of the method. The total coefficient of variation is 0.0869. Attachments include a brief report on the analysis of antimony using hydride evolution, a description of the vapor generation/dilution system, including diagrams, and a summary of statistical terms and formulae.
NIOSH-Author; NIOSH-Analytical-Method; Standards-Completion-Program; SCP; Analytical-Method; Standards; Sampling; Set-2; Air-quality-measurement; Air-sampling; Procedures; Antimony-compounds; Metal-compounds;
Division of Physical Sciences and Engineering, NIOSH, Cincinnati, Ohio, 27 pages, 8 references