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Colorimetric determination of siliceous atmospheric contaminants.
Talvitie NA; Hyslop F
Am Ind Hyg Assoc J 1958 Feb; 19(1):54-58
A method for colorimetric determination of siliceous atmospheric contaminants is described. Particulate silica (7631869) and silicates are collected on membrane filters, dissolved in hydrofluoric-acid (7664393), and determined colorimetrically as yellow silicomolybdate (11121258) or as molybdenum-blue (66771435) after reduction with 1-amino-2-naphthol-4-sulfonic-acid (116632). The dual sensitivity obtained by the use of the two colors permits accurate analyses in the relatively large range of 1 microgram to 2.5 milligrams without the necessity of taking an aliquot. The small air volumes required were easily sampled with hand-operated equipment.
NIOSH-Author; Methodology; Colorimetry; Assays; Pollution; Sulfonic-acids
N. A. Talvitie, Occupational Health Program, Bureau of State Services, Public Health Service, U. S. Department of Health, Education, and Welfare, lOl4 Broadway, Cincinnati, Ohio
7631-86-9; 7664-39-3; 11121-25-8; 66771-43-5; 116-63-2
Issue of Publication
American Industrial Hygiene Association Journal
Page last reviewed: November 6, 2020
Content source: National Institute for Occupational Safety and Health Education and Information Division