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An ultra-high-vacuum chamber for high-temperature X-ray diffractometry.

Authors
Krug-MP; McCune-RA; Romans-PA
Source
J Appl Crystallography 1971 Apr; 4(2):151-155
NIOSHTIC No.
10010200
Abstract
An attachment to a horizontal goniometer for x-ray powder diffraction at temperatures up to about 2,000 deg c in a vacuum in the 10-9 torr range is described. Specimen heating is by direct contact to a resistance strip heater with provision for electron beam heating. Temperature measurement is by thermocouple or optical pyrometer. High-temperature parameter measurements on vanadium are presented as one of the examples of the capability of the apparatus.
CODEN
JACGAR
Publication Date
19710401
Document Type
OP; Journal Article
Fiscal Year
1971
NTIS Accession No.
NTIS Price
Identifying No.
OP 138-71
Issue of Publication
2
ISSN
0021-8898
NIOSH Division
ALRC
Source Name
Journal of Applied Crystallography
State
OR
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