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NIOSH Analytical Methods for Set M.

Authors
Anonymous
Source
NIOSH 1976 Apr:66 pages
Link
NIOSHTIC No.
00133694
Abstract
Industrial hygiene sampling and analytical monitoring methods are presented for copper (7440508), mists and dusts, molybdenum (7439987) in soluble compounds, phthalic-anhydride (85449), rhodium (7440166) as metal fume and dust, zirconium (7440677) compounds, 2- hexanone (591786), phosphoric-acid (7664382), platinum (7440064) as soluble salts, and rhodium as soluble salts. The methods are validated under the joint NIOSH/OSHA Standards Completion Program for Set-M. For each compound, the analyte, matrix, OSHA standard, and validation date are given, and the method is described in terms of the principle of the method, range and sensitivity, interferences, precision and accuracy, advantages and disadvantages, apparatus, reagents, detailed procedure, analysis, sample recovery, calibration and standards, calculations, and references. Most compounds are collected by filter collection and analyses are by atomic absorption, gas or liquid chromatography, or colorimetry. The methods are verified as suitable for measuring airborne concentrations of the listed compounds, but other methods meeting the accuracy requirements may be used.
Keywords
NIOSH-Contract; Chemical-properties; Absorption-rates; Air-sampling-techniques; Industrial-hygiene; Air-sampling; Chromatographic-analysis; Analytical-instruments; Analytical-methods; Sampling-methods; Contract-099-74-0045;
CAS No.
7440-50-8; 7439-98-7; 85-44-9; 7440-16-6; 7440-67-7; 591-78-6; 7664-38-2; 7440-06-4;
Publication Date
19760401
Funding Type
Contract;
Fiscal Year
1976
NTIS Accession No.
PB-254228
NTIS Price
A05
Identifying No.
Contract-099-74-0045
Source Name
NIOSH, Public Health Service, U.S. Department of Health, Education, and Welfare, Cincinnati, Ohio, NTIS PB-254-228
State
OH;
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