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Failure Report No. S145.

Authors
Anonymous
Source
NIOSH 1977 Sep:5 pages
Link
NIOSHTIC No.
00107252
Abstract
Test results using the NIOSH analytical method S145 for ethylenediamine (107153) are reported. Two procedures were evaluated: collection on silica-gel (10193369), desorption with methanol (67561) and analysis by gas chromatography with a flame ionization detector; and collection in a midget bubble containing dilute acid, derivatization with fluorescamine, and analysis by high pressure liquid chromatography with a fluorescence detector. Analytical procedures are described. The first methods were unsatisfactory because of inadequate chromatographic resolution and insensitivity of the flame ionization detector. The second method did not provide sufficient stability of the fluorescent product.
Keywords
Phenyl-compounds; Gas-chromatography; High-pressure; Analytical-methods;
CAS No.
107-15-3; 10193-36-9; 67-56-1;
Publication Date
19770902
Fiscal Year
1977
NTIS Accession No.
PB81-230088
NTIS Price
A01
Source Name
NIOSH, Unpublished, Cincinnati, Ohio, 5 pages, 11 references
State
OH;
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