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NIOSH Analytical Method Pentachlorophenol Sampling Data Sheet No. S297.

Authors
NIOSH
Source
NIOSH 1977 Dec:.21 pages
Link
NIOSHTIC No.
00080936
Abstract
Data on collecting pentachlorophenol (87865) from air samples is given. Pentachlorophenol is collected by drawing 180 liters of air through a mixed cellulose ester membrane filter connected in series to a midget bubbler containing 15ml of ethylene-glycol (107211). A flow rate of 1.5 liters of air per minute is recommended. The filter is then disconnected and added to a bubbler flask. High pressure liquid chromatography is used to separate and analyze the pentachlorophenol. This method has been shown to be valid over the range of 0.2654 to 1.131mg/cu meter at 24 degrees-C and pressure of 761mm Hg (7439976). Needed sampling equipment includes: a calibrated personal sampling pump, a 37mm three piece filter holder; a 37mm diameter, 0.8 micrometer cellulose ester membrane, filter; Teflon and polyethylene tubing for sealing the bubbler stem. Recording information on other compounds present in the sampled air is recommended. Expeditious shipping of the samples to the laboratory is also recommended.
Keywords
NIOSH-Analytical-Method; Standards; Standards-Completion-Program; NIOSH-Contract; Contract-210-76-0123; Air-sampling-equipment; Alcohols; Herbicides; Phenolic-compounds; Analytical-Method; Chemical-groups; Sampling;
CAS No.
87-86-5; 107-21-1; 7439-97-6;
Publication Date
19771202
Funding Type
Contract;
Fiscal Year
1978
NTIS Accession No.
PB-288629
NTIS Price
Identifying No.
S297
NIOSH Division
DPSE;
Source Name
Division of Physical Sciences and Engineering, NIOSH, Cincinnati, Ohio
State
OH;
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