NIOSH Analytical Method, Tetramethyl Lead, Backup Data Report, S384, (Set 3).
NIOSH 1977 Nov:26 pages
Backup data are given for the analytical method for tetramethyl-lead (75741). The protocol for validation of the method consisted of the following: evaluation of capacity of various solid sorbents; analysis of 18 samples spiked with tetramethyl-lead; analysis of 18 samples collected from dynamically generated test atmospheres; determination of the breakthrough capacity of XAD-2 resin at high relative humidities; testing of the storage stability of collected samples; evaluation of sample migration during storage; and assessment of the precision and accuracy of the method.
NIOSH-Author; NIOSH-Analytical-Method; Standards-Completion-Program; Analytical-Method; Standards; Sampling; SCP; Set-3;
Division of Physical Sciences and Engineering, NIOSH, Cincinnati, Ohio, 26 pages, 5 references